Synthesis of 4-bromochalcone & 3-(4-bromophenyl)-5-phenylisoxazole

Appendix #3

Figure 18: IR spectrum of 4-bromochalcone

Integation 2 1 9

Figure 19: Proton NMR of 4-bromochalcone

Figure 20: Carbon-13 NMR of 4-bromochalcone

Figure 21: DEPT 45 of 4-bromochalcone

Figure 22: DEPT 90 of 4-bromochalcone

Figure 23: DEPT 135 of 4-bromochalcone

Figure 24: COSY of 4-bromochalcone

Figure 25: HETCOR of 4-bromochalcone

Figure 26: Mass Spectrum of 4-bromochalcone with match from spectral library

Appendix #4

Figure 27: Proton NMR of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Figure 28: Carbon-13 Spectrum of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Figure 29: DEPT 45 of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Figure 30: DEPT 90 of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one

Appendix #5

Figure 31: IR spectrum of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 32: Proton NMR of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 33: Carbon-13 NMR of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 34: DEPT 45 of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 35: DEPT 90 of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 36: DEPT 135 of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 37: COSY of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 38: HETCOR of 3-(4-bromophenyl)-5-phenylisoxazole

Figure 39: Mass Spectrum of 3-(4-bromophenyl)-5-phenylisoxazole