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Category : Natural Sciences

Enthalpy of Hydration

Written by Rachel Buckley Abstract This experiment, Enthalpy of Hydration, is used to calculate the enthalpy of hydration of magnesium sulfate by measuring the temperature change of both anhydrous magnesium sulfate and hydrated magnesium sulfate when they are added separately to two different calorimeters and allowed to react. The results are then used to calculate the enthalpy of hydration. Methods and Materials First, one sample of anhydrous, between 7 and 8 grams, and one sample of hydrate, between 15.3 and […]

Review of Basic Techniques and Purifying Proteins

Written by Kasia Bender Objectives: –       To practice calculating various solution components, including molarity and % (m/v). –       To practice the use of a graduated pipet and micropipette. –       To review lab safety. Part I A: Calculations   Part I B: Table One: Sample Conc. (µg/µL) glucose (µL) buffer (µL) 1 0.0 0.0 187.5 2 1.0 30.0 187.5 3 2.0 60.0 187.5 4 3.0 90.0 187.5 5 4.0 120.0 187.5 6 5.0 150.0 187.5 Table Two: Stock MM vol. MM […]

Synthesis of 4-bromochalcone & 3-(4-bromophenyl)-5-phenylisoxazole

Written by: Ryan Castellente Abstract An acylation reaction was performed reacting benzene with acetyl chloride, resulting in the 61% yield of acetophenone. An aldol condensation reaction reacted the acetophenone with 4-bromobenzaldehyde. This reaction produced 65% yield of 4-bromochalcone. A bromination reaction was performed on the 4-bromochalcone, resulting in a 76% yield of 2,3-dibromo-3-(4-bromophenyl)-1-phenylpropan-1-one. The final reaction formed an isoxazole ring, resulting in a 95% yield of 3-(4-bromophenyl)-5-phenylisoxazole. The synthesis scheme is seen below. Introduction Isoxazoles have been of interest to […]

Kinematic Linkage Systems: Analyzing Motion

Written by: Jeremy Stimack Introduction The analysis of the movement of a person has several powerful applications in determining the various biomechanical phenomena that occur within the body, such as joint motion or forces in the hip. Such information can provide valuable feedback in the research and development of medical devices that aid to remedy mechanical issues in affected individuals. Therefore, the objective of experimentation was to gain experience with a kinematic linkage system that is capable of measuring such […]

Electrochemistry Lab Experiment

Written by Elizabeth Data: Table 1: Measured Cell Potential Values Ecell (V) Cu/Zn 0.920 V Cu/Pb 0.646 V Zn/Pb 0.423 V   Table 2: Cell Potential Values for Reduction Half Reactions Ered (V) Cu2+ + 2e– –> Cu 0.34 V Zn2+ + 2e– –> Zn -0.58 V Pb2+ + 2e– –> Pb -0.31 V   Table 3: Elements of Cu/Pb Cell in Thermodynamic Study Temp (°C) Temp (K) ΔGrxn (kJ) Ecell (V) 76.0 °C 349 K -157.8 kJ 0.818 V 66.0 °C 339 K -158.8 kJ 0.823 V 56.0 […]

Synthesis and Spectroscopy of Eu(III) and Tb(III) diketonate complexes

Written by Alex Abstract The purpose of this experiment is to determine the electron energy transitions on Europium and Terbium complexes with tmh. This was determined by finding the wavelengths of the peaks in an emission spectrum of those complexes. It was found that the largest peak of the Europium complex was at 614 nm, and the largest peak of the Terbium complex was at 547 nm. Introduction In order to understand photochemistry, one must understand the basics of atomic […]